TY - JOUR
T1 - New efficient intercalation of bioactive molecules into layered double hydroxide materials by solid-state exchange
T2 - An in situ XRPD study
AU - Milanesio, Marco
AU - Conterosito, Eleonora
AU - Viterbo, Davide
AU - Perioli, Luana
AU - Croce, Gianluca
PY - 2010/11/3
Y1 - 2010/11/3
N2 - A new soft and fast solid state reaction is exploited for the preparation of exchanged layered double hydroxide materials and, in particular, for intercalating bioactive molecules. The characterization of the nanocomposite, carried out by crystallographic and thermogravimetric techniques, revealed that this synthesis yield is comparable to that of standard methods but with time, solvent, and energy saving advantages. Moreover, the in situ diffraction experiments also allowed us to shed some light on the kinetics of the intercalation process.
AB - A new soft and fast solid state reaction is exploited for the preparation of exchanged layered double hydroxide materials and, in particular, for intercalating bioactive molecules. The characterization of the nanocomposite, carried out by crystallographic and thermogravimetric techniques, revealed that this synthesis yield is comparable to that of standard methods but with time, solvent, and energy saving advantages. Moreover, the in situ diffraction experiments also allowed us to shed some light on the kinetics of the intercalation process.
UR - http://www.scopus.com/inward/record.url?scp=78149337953&partnerID=8YFLogxK
U2 - 10.1021/cg1011023
DO - 10.1021/cg1011023
M3 - Article
SN - 1528-7483
VL - 10
SP - 4710
EP - 4712
JO - Crystal Growth and Design
JF - Crystal Growth and Design
IS - 11
ER -