One-step synthesis of a new eight-membered cyclic ligand from glycine, formaldehyde and hypophosphorous acid

Silvio Aime; Camilla Cavallotti; Eliana Gianolio; Giovanni B. Giovenzana; Giovanni Palmisano; Massimo Sisti

doi:10.1016/S0040-4039(02)01950-0

One-step synthesis of a new eight-membered cyclic ligand from glycine, formaldehyde and hypophosphorous acid

Silvio Aime, Camilla Cavallotti, Eliana Gianolio, Giovanni B. Giovenzana, Giovanni Palmisano, Massimo Sisti

Department of Pharmaceutical Sciences

Research output: Contribution to journal › Article › peer-review

Abstract

The eight-membered 3,7-dihydroxy-3,7-dioxoperhydro-1,5,3,7-diazadiphosphocine-1,5-diacetic acid was obtained with a one-step reaction of glycine, formaldehyde and hypophosphorous acid in acidic aqueous medium. A preliminary investigation of its coordination properties is reported.

Original language	English
Pages (from-to)	8387-8389
Number of pages	3
Journal	Tetrahedron Letters
Volume	43
Issue number	46
DOIs	https://doi.org/10.1016/S0040-4039(02)01950-0
Publication status	Published - 11 Nov 2002

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title = "One-step synthesis of a new eight-membered cyclic ligand from glycine, formaldehyde and hypophosphorous acid",

abstract = "The eight-membered 3,7-dihydroxy-3,7-dioxoperhydro-1,5,3,7-diazadiphosphocine-1,5-diacetic acid was obtained with a one-step reaction of glycine, formaldehyde and hypophosphorous acid in acidic aqueous medium. A preliminary investigation of its coordination properties is reported.",

author = "Silvio Aime and Camilla Cavallotti and Eliana Gianolio and Giovenzana, \{Giovanni B.\} and Giovanni Palmisano and Massimo Sisti",

note = "Funding Information: Financial support from Bracco Imaging (Milan) and Italian CNR (Target Project on Biotechnology) is gratefully acknowledged. Two of the authors (C.C. and M.S.) are thankful to Dipartimento di Chimica Organica e Industriale, Universit{\`a} degli Studi, Milan) for their kind hospitality in their laboratories. ",

year = "2002",

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day = "11",

doi = "10.1016/S0040-4039(02)01950-0",

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volume = "43",

pages = "8387--8389",

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TY - JOUR

T1 - One-step synthesis of a new eight-membered cyclic ligand from glycine, formaldehyde and hypophosphorous acid

AU - Aime, Silvio

AU - Cavallotti, Camilla

AU - Gianolio, Eliana

AU - Giovenzana, Giovanni B.

AU - Palmisano, Giovanni

AU - Sisti, Massimo

N1 - Funding Information: Financial support from Bracco Imaging (Milan) and Italian CNR (Target Project on Biotechnology) is gratefully acknowledged. Two of the authors (C.C. and M.S.) are thankful to Dipartimento di Chimica Organica e Industriale, Università degli Studi, Milan) for their kind hospitality in their laboratories.

PY - 2002/11/11

Y1 - 2002/11/11

N2 - The eight-membered 3,7-dihydroxy-3,7-dioxoperhydro-1,5,3,7-diazadiphosphocine-1,5-diacetic acid was obtained with a one-step reaction of glycine, formaldehyde and hypophosphorous acid in acidic aqueous medium. A preliminary investigation of its coordination properties is reported.

AB - The eight-membered 3,7-dihydroxy-3,7-dioxoperhydro-1,5,3,7-diazadiphosphocine-1,5-diacetic acid was obtained with a one-step reaction of glycine, formaldehyde and hypophosphorous acid in acidic aqueous medium. A preliminary investigation of its coordination properties is reported.

UR - https://www.scopus.com/pages/publications/0037064481

U2 - 10.1016/S0040-4039(02)01950-0

DO - 10.1016/S0040-4039(02)01950-0

M3 - Article

SN - 0040-4039

VL - 43

SP - 8387

EP - 8389

JO - Tetrahedron Letters

JF - Tetrahedron Letters

IS - 46

ER -

One-step synthesis of a new eight-membered cyclic ligand from glycine, formaldehyde and hypophosphorous acid

Abstract

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